化工社化工社 化学情報印刷レポート · 研究参考用
2-(Trifluoromethyl)acrylic acid → 3-Acetylthio-2-trifluoromethylpropanoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Trifluoromethyl)acrylic acid | HCID 587694 | — |
| 反応物 | HCID 178473673 | HCID 178473673 | — |
| 生成物 | 3-Acetylthio-2-trifluoromethylpropanoic acid | HCID 12833014 | — |
反応手順
A mixture of thiolactic acid (50 g.) and 2-(trifluoromethyl)acrylic acid [M. W. Buxton, et al., J. Chem. Soc., 366 (1954)] (66 g.) is heated on the steam bath for one hour and then stored at room temperature for eighteen hours. The reaction mixture is distilled in vacuo to give 3-acetylthio-2-trifluoromethylpropanoic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04734420 |
| 出典データセット | uspto-grants-1988_03 |
| ORD ID | ord-f1430a46860347daae74740f3bca9852 |
| 出典メモ | uspto-grants-1988_03 |