Methanol → HCID 178434169, compound

HRID 569921Notes

Reaction equation

HRID 569921 reaction equation
[CH3:1][C:2]1[C:3]2[CH:14]=[CH:13][C:8]3[NH:9][N:10]=[C:11](C)[C:7]=3[C:4]=2[NH:5][N:6]=1.[CH3:15]O>>[CH3:1][C:2]1[C:3]2[CH:14]=[CH:13][C:8]3[N:9]([CH3:15])[N:10]=[CH:11][C:7]=3[C:4]=2[NH:5][N:6]=1

Participants

3

Reactant 2

HCID 887MethanolHCID 178434173HCID 178434173, compound

Product 1

HCID 178434169HCID 178434169, compoundYield 70%

Procedure

1,6-Dihydro-3,8-dimethylbenzo[1,2-c:3,4-c']dipyrazole as a light-lavender powder melting at above 290° C. The product powder (70% yield) was obtained by trituration of the crude product in hot methanol followed by cooling.

Sources & evidence

ORD record
ord-2f58f6a6ff3945b3b10fd390e01a1a66
Source dataset
uspto-grants-1988_03
Patent number
US04734430

Reaction notes

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