HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 117622627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 117622672 | HCID 117622672 | — |
| Product | HCID 117622627 | HCID 117622627 | — |
Reaction Steps
127 mg (0.23 mmol) of tert-butyl 4-({2-[4-(5-chloro-2-cyanophenyl)-5-methoxy-2-oxopyridin-1(2H)-yl]-4-methylpentanoyl}amino)benzoate (racemate) (Example 25.1C) were hydrolysed with TFA according to General Method 2. Yield: 79 mg (71% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434690B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-77a412704818411cb7caecfaf16bc476 |
| Source note | uspto-grants-2016_09 |