HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(Diphenyl-lambda~4~-sulfanylidene)-4-methylbenzene-1-sulfonamide → HCID 86742071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(Diphenyl-lambda~4~-sulfanylidene)-4-methylbenzene-1-sulfonamide | HCID 264695 | — |
| Reactant | Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) | HCID 2735153 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86742071 | HCID 86742071 | — |
Reaction Steps
10.65 g (0.03 mol) of N-p-toluenesulfonyldiphenylsulfilimine were dissolved in 40 ml of dry methylene chloride, and 4.44 g (0.03 mol) of trimethyloxonium tetrafluoroborate were added. After stirring overnight and concentrating, the reaction product formed a crystalline precipitate. Drying under reduced pressure left 11.45 g of the salt (IV). Analysis and properties are indicated in Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04734444 |
| Source dataset | uspto-grants-1988_03 |
| ORD ID | ord-7a173d6a431d4904a5adb43c0a63eb8a |
| Source note | uspto-grants-1988_03 |