3-Methoxyphenethylamine → HCID 50924143, compound

Participants

Reaction Steps

This compound was prepared in an analogous manner as 3-{[3-(1H-Pyrrolo[2,3-b]pyridin-4-ylamino)-thiophene-2-carbonyl]-amino}-pyrrolidine-1-carboxylic acid tert-butyl ester using 2-(3-methoxyphenyl)ethylamine instead of 1-BOC-3-aminopyrrolidine. LCMS (ESI) 393 (M+H) 1H NMR (400 MHz, DMSO-d6) δ ppm 11.68 (1H, br. s.) 10.34 (1H, s) 8.19 (1H, t, J=5.61 Hz) 8.03 (1H, d, J=5.66 Hz) 7.79 (1H, d, J=5.37 Hz) 7.45 (1H, d, J=5.37 Hz) 7.34 (1H, d, J=3.32 Hz) 7.16 (1H, t, J=8.10 Hz) 6.72-6.82 (4H, m) 6.48 (1H, d, J=3.32 Hz) 3.71 (3H, s) 3.46 (2H, dt, J=8.00, 6.25 Hz) 2.79 (2H, t, J=7.27 Hz)

Provenance & Evidence