Acetophenone → HCID 70795517, compound

Participants

Reaction Steps

This compound was prepared in an analogous manner as 3-(1H-Pyrrolo[2,3-b]pyridin-4-ylamino)-thiophene-2-carboxylic acid [2-(4-methoxy-benzylamino)-ethyl]amide using acetophenone instead of 4-methoxy benzaldehyde. LCMS (ESI) 406 (M+H) 1H NMR (400 MHz, DMSO-d6) δ ppm 11.53 (1H, br. s.) 10.22 (1H, s) 8.02 (2H, d, J=5.37 Hz) 7.76 (1H, d, J=5.37 Hz) 7.45 (1H, d, J=5.47 Hz) 7.21-7.34 (5H, m) 7.08-7.20 (1H, m) 6.79 (1H, d, J=5.37 Hz) 6.43 (1H, d, J=2.73 Hz) 3.67 (1H, q, J=6.51 Hz) 3.18-3.38 (2H, m) 2.34-2.58 (2H, m) 2.14 (1H, br. s.) 1.19 (3H, d, J=6.64 Hz)

Provenance & Evidence