Ethynylcyclohexane → HCID 46892773, compound

HRID 570664Notes

Reaction equation

HRID 570664 reaction equation
[N:1]([CH:4]1[CH2:23][N:8]2[C:9]3[C:14]([C:15]([CH2:16][C:17]([O:19]CCC)=[O:18])=[C:7]2[CH2:6][CH2:5]1)=[CH:13][CH:12]=[CH:11][CH:10]=3)=[N+:2]=[N-:3].[C:24]([CH:26]1[CH2:31][CH2:30][CH2:29][CH2:28][CH2:27]1)#[CH:25]>>[CH:26]1([C:24]2[N:1]([CH:4]3[CH2:23][N:8]4[C:9]5[C:14]([C:15]([CH2:16][C:17]([OH:19])=[O:18])=[C:7]4[CH2:6][CH2:5]3)=[CH:13][CH:12]=[CH:11][CH:10]=5)[N:2]=[N:3][CH:25]=2)[CH2:31][CH2:30][CH2:29][CH2:28][CH2:27]1

Participants

3

Reactant 2

HCID 70263EthynylcyclohexaneHCID 59487226Propyl (7-azido-6,7,8,9-tetrahydropyrido[1,2-a]indol-10-yl)acetate

Product 1

HCID 46892773HCID 46892773, compound

Procedure

The title compound was prepared using procedures described in EXAMPLE 3 from propyl (7-azido-6,7,8,9-tetrahydropyrido[1,2-α]indol-10-yl)acetate and ethynylcyclohexane. MS (+ESI) m/z: 379.2.

Sources & evidence

ORD record
ord-3d7c5e8a85c3457cb7f31847c6989345
Source dataset
uspto-grants-2015_05
Patent number
US09023864B2

Reaction notes

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