Carbon tetrabromide → HCID 49868873, compound

Participants

Reaction Steps

N′-Benzoyl-3-methyl-4-oxo-3,4-dihydroimidazo[5,1-d][1,2,3,5]tetrazine-8-carbohydrazide (0.03 mmol), carbon tetrabromide (0.06 mmol) and triphenylphosphine (0.06 mmol) were stirred in DCM (0.5 mL) for 3 hours. The crude reaction mixture was purified by column chromatography, eluting with 10% MeCN/DCM, to give the title compound. δH (DMSO-d6) 9.06 (1H, s), 8.11 (2H, m), 7.67 (3H, m), 3.93 (3H, s).

Provenance & Evidence