Methyl N-(triethylammoniosulfonyl)carbamate → HCID 49868874, compound

Participants

Reaction Steps

N′-Benzoyl-4-oxo-3-(prop-2-ynyl)-3,4-dihydroimidazo[5,1-d][1,2,3,5]tetrazine-8-carbohydrazide (0.15 mmol) and Burgess reagent (0.30 mmol) were heated under microwave irradiation in THF (1 mL) at 60° C. for 2 minutes (Max Power 100 W). The precipitate was filtered and washed with DCM to give the title compound. δH (DMSO-d6) 9.10 (1H, s), 8.13 (2H, m), 7.70 (3H, m), 5.20 (2H, d, J=2.8), 3.57 (1H, t, J=2.8).

Provenance & Evidence