3-Iodo-4-methylbenzoic acid → HCID 86701366, compound

HRID 570978Notes

Reaction equation

HRID 570978 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[CH3:11])[C:5]([OH:7])=O.[Cl:12][C:13]1[CH:22]=[C:21]([Cl:23])[CH:20]=[C:19]([Cl:24])[C:14]=1[C:15]([NH:17][NH2:18])=[O:16]>>[I:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[CH3:11])[C:5]([N:17]([C:15](=[O:16])[C:14]1[C:19]([Cl:24])=[CH:20][C:21]([Cl:23])=[CH:22][C:13]=1[Cl:12])[NH2:18])=[O:7]

Participants

3

Reactant 2

HCID 6216403-Iodo-4-methylbenzoic acidHCID 21973562HCID 21973562, compound

Product 1

HCID 86701366HCID 86701366, compound

Procedure

N-(3-iodo-4-methylbenzoyl)-2,4,6-trichlorobenzohydrazide was prepared by the reaction of 3-iodo-4-methylbenzoic acid with 2,4,6-trichlorobenzohydrazide. The coupling was performed in a manner similar to that described in Reference Example 3.

Sources & evidence

ORD record
ord-797014c0818a4e8c8887eed515ab8d79
Source dataset
uspto-grants-2015_05
Patent number
US09024021B2

Reaction notes

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