HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,7-Dichloro-2,9-dimethyl-1,10-phenanthroline → HCID 89612430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,7-Dichloro-2,9-dimethyl-1,10-phenanthroline | HCID 10588548 | — |
| Reactant | HCID 178444609 | HCID 178444609 | — |
| Product | HCID 89612430 | HCID 89612430 | — |
Reaction Steps
4,7-dichloro-2,9-dimethyl-1,10-phenanthroline, Phen1, is synthesized according to the literature (M. Schmittel, H. Ammon Eur. J. Org. Chem. 1998, 785.). For the substitution with a n-butyl group, an equimolar amount of n-HexMgBr and CuBr is added. The purification of Phen2 is done using column chromatography over silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09024026B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-69d0660ff770430b95871bc780f8e4fb |
| Source note | uspto-grants-2015_05 |