HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hexylphenylboronic Acid → 2,9-Dimethyl-4,7-di-(p-hexylphenyl)-1,10-phenanthroline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hexylphenylboronic Acid | HCID 4197864 | — |
| Reactant | 4,7-Dibromo-2,9-dimethyl-1,10-phenanthroline | HCID 10522896 | — |
| Product | 2,9-Dimethyl-4,7-di-(p-hexylphenyl)-1,10-phenanthroline | HCID 68013875 | — |
Reaction Steps
Starting with 4,7-dibromo-2,9-dimethyl-1,10-phenanthroline, Phen8, (M. Schmittel, H. Ammon Eur. J. Org. Chem. 1998, 785) and the p-hexylphenylboronic acid (commercially available), the ligand Phen9 is synthesized by a Suzuki-coupling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09024026B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-95498c742a2f43e3a588c85032ba20f6 |
| Source note | uspto-grants-2015_05 |