Hydrogen Peroxide → HCID 86660798, compound

Participants

Reaction Conditions

Reaction Steps

A 100 mL reactor was charged with 11.5 g (26% purity, 0.012 mole/1.0 equivalent) of triethylammonium 1,1-difluoro-2-hydroxy-ethane-1-sulfinate, 20 g of water and 4.2 g (0.036 mole/3.0 equivalents) of 30% hydrogen peroxide at room temperature, followed by one day of stirring at 40° C. Upon confirming the termination of the reaction, the reaction liquid underwent cooling. Thereafter, the reaction liquid was subjected to distillation of the solvent and brought into dryness, thereby obtaining 10.5 g of a target triethylammonium 1,1-difluoro-2-hydroxy-ethane-1-sulfonate. It exhibited a purity of 26% and a yield of 85% at this time.

Provenance & Evidence