HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Solketal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Glycerol | HCID 753 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Water | HCID 962 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Solketal | HCID 7528 | — |
Reaction Steps
A similar experiment to that of example 1 is carried out using this time 2 kg of crude product comprising 42% by weight of glycerol, 14% by weight of water and a large amount of volatile products (methanol, ethanol). The acetone is used in the same molar ratio as is for example 1 and the 2,2-dimethyl-1,3-dioxolane-4-methanol obtained has a purity of 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09024081B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-c3d8243c032c4459b3eaf6724bebf426 |
| Source note | uspto-grants-2015_05 |