HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 86697864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | tert-butyl 2-bromo-4H,5H,6H,7H,8H-(1,3)thiazolo(4,5-d)azepine-6-carboxylate | HCID 71651202 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86697864 | HCID 86697864 | — |
Reaction Steps
1.00 g (3.00 mmol) bromo-4,5,7,8-tetrahydro-thiazolo[4,5-d]azepine-6-carboxylic acid tert-butyl ester, 0.40 g (7.00 mmol) sodium methylate in 15 mL methanol were heated at 100° C. for 4 h under microwave irradiation. The mixture was purified by chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029360B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-e0578dacedec4d328ea8746c99d34f47 |
| Source note | uspto-grants-2015_05 |