HRID571639
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The title compound was prepared in accordance with the general method of example 1 from 6-bromo-pyrazolo[1,5-A]pyrimidine-2-carboxylic acid and 2-methyl-5,6,7,8-tetrahydro-4H-thiazolo[4,5-d]azepine hydrochloride. The reaction mixture was purified by HPLC chromatography and lyophilized. Yield: 13 mg (16% of theory). ESI-MS: m/z=392 (M+H)+;
WORKUP
后处理
- customThe reaction mixture was purified by HPLC chromatography