HRID571639

反应详情

EQUATION

反应方程式

HRID 571639 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in accordance with the general method of example 1 from 6-bromo-pyrazolo[1,5-A]pyrimidine-2-carboxylic acid and 2-methyl-5,6,7,8-tetrahydro-4H-thiazolo[4,5-d]azepine hydrochloride. The reaction mixture was purified by HPLC chromatography and lyophilized. Yield: 13 mg (16% of theory). ESI-MS: m/z=392 (M+H)+;

WORKUP

后处理

  1. customThe reaction mixture was purified by HPLC chromatography