HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Tris(1-methylethyl)benzenesulfonyl chloride → tert-butyl ((1R,3S)-3-{[(2,4,6-triisopropylphenyl)sulfonyl]amino}cyclohexyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Tris(1-methylethyl)benzenesulfonyl chloride | HCID 81042 | — |
| Reactant | rac-tert-butyl N-((1R,3S)-3-aminocyclohexyl)carbamate | HCID 59710757 | — |
| Product | tert-butyl ((1R,3S)-3-{[(2,4,6-triisopropylphenyl)sulfonyl]amino}cyclohexyl)carbamate | HCID 69756926 | — |
Reaction Steps
Compound 7b was prepared following procedures similar to those described previously in Example 1, step A, substituting 7a for i-2d and 2,4,6-triisopropylbenzenesulfonyl chloride for i-5f, respectively. m/z (ES) 503 (MH+Na)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029377B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-7ac57cda3ad544349c66f6225cec49ac |
| Source note | uspto-grants-2015_05 |