HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 58522792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 58522750 | HCID 58522750 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58522792 | HCID 58522792 | — |
Reaction Steps
To a solution of example 133 (25 mg) in anhydrous THF (1 mL), a 1M solution of TBAF in THF (100 μL, 2.0 equiv.) was added. The reaction mixture was heated at reflux for 1 Hr, then was concentrated under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029393B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-bc76965f1f1e4a5783ec775262cc6dfc |
| Source note | uspto-grants-2015_05 |