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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 572167Generated: October 31, 2026

HCID 86704975, compound → HCID 86704978, compound

https://huagongshe.com/reaction/572167

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86704975HCID 86704975—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 86704978HCID 8670497862.4%

Reaction Steps

A suspension of 1-[4-(benzyloxy)phenyl]-3-methoxy-1H-pyrazolo[3,4-b]pyridine (1.1 g) and 10% palladium on carbon (containing water (50%), 0.10 g) in methanol (50 ml) was stirred for 3 hr under a hydrogen atmosphere at room temperature. The reaction mixture was filtered through celite, and the filtrate was purified by silica gel column chromatography (hexane/ethyl acetate) to give the title compound (0.50 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09029388B2
Source datasetuspto-grants-2015_05
ORD IDord-89a34f337491435ebb79d362bcd2016e
Source noteuspto-grants-2015_05