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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 572758Generated: November 3, 2026

2,3-Dichloroaniline → HCID 58234998, compound

https://huagongshe.com/reaction/572758

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,3-DichloroanilineHCID 11844—
Reactant8-(1-bromoethyl)-N,N-dimethyl-2-morpholino-4-oxo-4H-chromene-6-carboxamide hydrobromideHCID 67103675—
ProductHCID 58234998HCID 5823499852%

Reaction Steps

2,3-dichloroaniline (0.097 mL, 0.82 mmol) was reacted with 8-(1-bromoethyl)-N,N-dimethyl-2-morpholino-4-oxo-4H-chromene-6-carboxamide hydrobromide (0.1 g, 0.20 mmol) using an analogous procedure to the one described in Example 3.03 to give 8-(1-(2,3-dichlorophenylamino)ethyl)-N,N-dimethyl-2-morpholino-4-oxo-4H-chromene-6-carboxamide (51 mg, 51%) as a white solid. Mass Spectrum: M+H+ 490.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09029374B2
Source datasetuspto-grants-2015_05
ORD IDord-2c5e2b94bbd84ee78a62c16ceaa744d5
Source noteuspto-grants-2015_05