HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dichloroaniline → HCID 58234998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dichloroaniline | HCID 11844 | — |
| Reactant | 8-(1-bromoethyl)-N,N-dimethyl-2-morpholino-4-oxo-4H-chromene-6-carboxamide hydrobromide | HCID 67103675 | — |
| Product | HCID 58234998 | HCID 58234998 | 52% |
Reaction Steps
2,3-dichloroaniline (0.097 mL, 0.82 mmol) was reacted with 8-(1-bromoethyl)-N,N-dimethyl-2-morpholino-4-oxo-4H-chromene-6-carboxamide hydrobromide (0.1 g, 0.20 mmol) using an analogous procedure to the one described in Example 3.03 to give 8-(1-(2,3-dichlorophenylamino)ethyl)-N,N-dimethyl-2-morpholino-4-oxo-4H-chromene-6-carboxamide (51 mg, 51%) as a white solid. Mass Spectrum: M+H+ 490.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029374B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-2c5e2b94bbd84ee78a62c16ceaa744d5 |
| Source note | uspto-grants-2015_05 |