HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 10796784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 86719089 | HCID 86719089 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 10796784 | HCID 10796784 | — |
Reaction Steps
To a solution of cyclobutane-1,3-diylbis(methylene)bis(4-methylbenzenesulfonate) I-13 (1 equivalent) in DMF was added NaCN (6 equivalents) and was refluxed for 12 h. During workup, the reaction mixture was diluted with water and the desired compound was extracted with ethyl acetate. Evaporation of the organic solvent furnished I-14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029531B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-9c4bb98855394cdebeb135ea15100892 |
| Source note | uspto-grants-2015_05 |