Dimethylamine → HCID 178434643, compound

HRID 57302Notes

Reaction equation

HRID 57302 reaction equation
Br[CH2:2][C:3]1[CH:18]=[CH:17][C:6]2[N:7]=[C:8]([C:10]3[C:14]([CH3:15])=[N:13][NH:12][C:11]=3[NH2:16])[S:9][C:5]=2[CH:4]=1.[CH3:19][NH:20][CH3:21]>>[CH3:19][N:20]([CH2:2][C:3]1[CH:18]=[CH:17][C:6]2[N:7]=[C:8]([C:10]3[C:14]([CH3:15])=[N:13][NH:12][C:11]=3[NH2:16])[S:9][C:5]=2[CH:4]=1)[CH3:21]

Participants

3

Reactant 2

HCID 674DimethylamineHCID 178434639HCID 178434639, compound

Product 1

HCID 178434643HCID 178434643, compound

Procedure

The title compound (24 mg) was prepared starting from 40 mg of 4-(6-bromomethylbenzothiazol-2-yl)-5-methyl-2H-pyrazol-3-ylamine and excess dimethylamine. MS (m/z, ES+): 288.1 (M+1, 20%), 243.1 (M−(CH3)2N, 100%).

Sources & evidence

ORD record
ord-d4fe3f0e2cef48cc865d2a45f781b876
Source dataset
uspto-grants-2016_09
Patent number
US09434720B2

Reaction notes

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