Ethanolamine → HCID 178434644, compound

HRID 57303Notes

Reaction equation

HRID 57303 reaction equation
Br[CH2:2][C:3]1[CH:18]=[CH:17][C:6]2[N:7]=[C:8]([C:10]3[C:14]([CH3:15])=[N:13][NH:12][C:11]=3[NH2:16])[S:9][C:5]=2[CH:4]=1.[NH2:19][CH2:20][CH2:21][OH:22]>>[NH2:16][C:11]1[NH:12][N:13]=[C:14]([CH3:15])[C:10]=1[C:8]1[S:9][C:5]2[CH:4]=[C:3]([CH2:2][NH:19][CH2:20][CH2:21][OH:22])[CH:18]=[CH:17][C:6]=2[N:7]=1

Participants

3

Reactant 2

HCID 700EthanolamineHCID 178434639HCID 178434639, compound

Product 1

HCID 178434644HCID 178434644, compound

Procedure

The title compound (10 mg) was prepared starting from 40 mg of 4-(6-bromomethylbenzothiazol-2-yl)-5-methyl-2H-pyrazol-3-ylamine and excess 2-aminoethanol. MS (m/z, ES+): 304.1 (M+1, 10%), 243.2 (M-HOCH2CH2NH, 100%).

Sources & evidence

ORD record
ord-38ba41b677f44107b87d40c336e41dee
Source dataset
uspto-grants-2016_09
Patent number
US09434720B2

Reaction notes

Loading…