HRID573160

反应详情

EQUATION

反应方程式

HRID 573160 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of EXAMPLE 368B (1.1 g) in methanol was hydrogenated over Raney Ni, at 60 psi of H2 at room temperature. The filtered solution was concentrated to give the title compound.

WORKUP

后处理

  1. concentrationThe filtered solution was concentrated