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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 573195Generated: October 30, 2026

HCID 67227683, compound → HCID 136344873, compound

https://huagongshe.com/reaction/573195

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67227683HCID 67227683—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 136344873HCID 136344873—

Reaction Steps

A mixture of EXAMPLE 419C (1.25 g) and 5% palladium on carbon (0.35 g) in ethanol (20 mL) was treated with a balloon of hydrogen. The reaction mixture was stirred overnight. The solid was filtered off. The filtrate was concentrated. The residue was purified by flash chromatography on silica gel to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09029404B2
Source datasetuspto-grants-2015_05
ORD IDord-57170aceedd04bc89342288fff692ea9
Source noteuspto-grants-2015_05