Water → HCID 66728128, compound

Participants

Reaction Steps

A mixture of 3-[(1-(1H-benzo[d]imidazol-2-yl)-1H-pyrazol-4-yl]-1-ethyl-1H-pyrazolo[4,3-b]pyridine (8 mg), MeI (2.278 μL) and Cs2CO3 (15.83 mg) in DMF (2 mL) was stirred at room temperature for 3 h, treated with water, and extracted with AcOEt. The organic layer was dried over MgSO4 and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (AcOEt/hexane). Crystallization from AcOEt/hexane gave the title compound (4.80 mg).

Provenance & Evidence