HRID573354

反应详情

EQUATION

反应方程式

HRID 573354 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 3-[4-(benzyloxy)phenyl]-6-fluoro-1-(1-methylethyl)-1H-pyrazolo[4,3-b]pyridine (130 mg) and 10% Pd—C (100 mg) in EtOH (20 mL) was stirred at room temperature for 1 h under H2 atmosphere, filtered and evaporated. The residue was purified by silica gel column chromatography (hexane/AcOEt) to give the title compound (76 mg).

WORKUP

后处理

  1. filtrationfiltered
  2. customevaporated
  3. customThe residue was purified by silica gel column chromatography (hexane/AcOEt)