HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68380244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 6-Phenylpyridine-3-sulfonyl chloride | HCID 24229463 | — |
| Reactant | HCID 68324013 | HCID 68324013 | — |
| Product | HCID 68380244 | HCID 68380244 | — |
Reaction Steps
Following general method outlined in Example 52, starting from 6-methyl-2-(1-methylethyl)-3-[3-(methyloxy)phenyl]thieno[2,3-b]pyridin-4-amine (40 mg, 0.128 mmol) (Description 21) and 6-phenyl-3-pyridinesulfonyl chloride (39 mg, 0.154 mmol), the title compound (12.2 mg) was isolated as a TFA salt. LCMS (B) m/z: 530 [M+1]+, Rt 3.02 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09029545B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-673b0e8b47294e6e98784032b93157ec |
| Source note | uspto-grants-2015_05 |