HCID 4635987, compound → HCID 25100046, compound

HRID 574706Notes

Reaction equation

HRID 574706 reaction equation
[N:1]([C:4]1[S:8][C:7]2[CH2:9][CH:10]([CH3:13])[CH2:11][CH2:12][C:6]=2[C:5]=1[C:14]([O:16]C)=O)=[C:2]=[S:3].[CH3:18][C:19]1[N:23]([CH2:24][CH2:25][CH2:26][NH2:27])[CH:22]=[N:21][CH:20]=1>>[CH3:13][CH:10]1[CH2:11][CH2:12][C:6]2[C:5]3[C:14](=[O:16])[N:27]([CH2:26][CH2:25][CH2:24][N:23]4[C:19]([CH3:18])=[CH:20][N:21]=[CH:22]4)[C:2](=[S:3])[NH:1][C:4]=3[S:8][C:7]=2[CH2:9]1

Participants

3

Reactant 2

HCID 4635987HCID 4635987, compoundHCID 194294833-(5-methyl-1H-imidazol-1-yl)propan-1-amine

Product 1

HCID 25100046HCID 25100046, compound

Procedure

The compound was synthesized starting from methyl 4,5,6,7-tetrahydro-2-isothiocyanato-6-methylbenzo[b]thiophene-3-carboxylate (0.10 g, 0.37 mmol) and 3-(5-methyl-1H-imidazol-1-yl)propan-1-amine (5) (0.052 g, 0.37 mmol) as described above.

Workup

  1. customThe compound was synthesized

Sources & evidence

ORD record
ord-ee8ad6a145ca405587ec21d82c8d7c14
Source dataset
uspto-grants-2015_05
Patent number
US09034907B2

Reaction notes

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