HCID 3251003, compound → HCID 25100199, compound

HRID 574708Notes

Reaction equation

HRID 574708 reaction equation
[N:1]([C:4]1[S:8][C:7]2[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:6]=2[C:5]=1[C:15]([O:17]C)=O)=[C:2]=[S:3].[CH3:19][C:20]1[N:24]([CH2:25][CH2:26][CH2:27][NH2:28])[CH:23]=[N:22][CH:21]=1>>[CH3:19][C:20]1[N:24]([CH2:25][CH2:26][CH2:27][N:28]2[C:15](=[O:17])[C:5]3[C:6]4[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][C:7]=4[S:8][C:4]=3[NH:1][C:2]2=[S:3])[CH:23]=[N:22][CH:21]=1

Participants

3

Reactant 2

HCID 3251003HCID 3251003, compoundHCID 194294833-(5-methyl-1H-imidazol-1-yl)propan-1-amine

Product 1

HCID 25100199HCID 25100199, compound

Procedure

The compound was synthesized starting from methyl 4,5,6,7,8,9-hexahydro-2-isothiocyanatocycloocta[b]thiophene-3-carboxylate (0.10 g, 0.36 mmol) and 3-(5-methyl-1H-imidazol-1-yl)propan-1-amine (5) (0.049 g, 0.36 mmol) as described above.

Workup

  1. customThe compound was synthesized

Sources & evidence

ORD record
ord-7a0a69f21f224cab86adbdc53e3aaf2d
Source dataset
uspto-grants-2015_05
Patent number
US09034907B2

Reaction notes

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