HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-isothiocyanato-4,5-dimethylthiophene-3-carboxylate → 2,3-dihydro-5,6-dimethyl-3-(3-(4-methyl-1H-imidazol-1-yl)propyl)-2-thioxothieno[2,3-d]pyrimidin-4(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-isothiocyanato-4,5-dimethylthiophene-3-carboxylate | HCID 3459267 | — |
| Reactant | 3-(4-Methyl-1H-imidazol-1-yl)propan-1-amine | HCID 15034954 | — |
| Product | 2,3-dihydro-5,6-dimethyl-3-(3-(4-methyl-1H-imidazol-1-yl)propyl)-2-thioxothieno[2,3-d]pyrimidin-4(1H)-one | HCID 25100358 | — |
Reaction Steps
The compound was synthesized starting from methyl 2-isothiocyanato-4,5-dimethylthiophene-3-carboxylate (0.100 g. 0.44 mmol) and 3-(4-methyl-1H-imidazol-1-yl)propan-1-amine (9) (0.061 g, 0.44 mmol) as described above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09034907B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-52095c895e9d4e89808dc992f164273e |
| Source note | uspto-grants-2015_05 |