HCID 3264560, compound → HCID 25100360, compound
Reaction equation
[N:1]([C:4]1[S:5][C:6]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:7][C:8]=1[C:9]([O:11]C)=O)=[C:2]=[S:3].[CH3:19][C:20]1[N:21]=[CH:22][N:23]([CH2:25][CH2:26][CH2:27][NH2:28])[CH:24]=1>>[CH3:19][C:20]1[N:21]=[CH:22][N:23]([CH2:25][CH2:26][CH2:27][N:28]2[C:9](=[O:11])[C:8]3[CH:7]=[C:6]([C:13]4[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=4)[S:5][C:4]=3[NH:1][C:2]2=[S:3])[CH:24]=1Participants
3
Procedure
The compound was synthesized starting from methyl 2-isothiocyanato-5-phenylthiophene-3-carboxylate (0.107 g. 0.39 mmol) and 3-(4-methyl-1H-imidazol-1-yl)propan-1-amine (9) (0.054 g, 0.39 mmol) as described above.
Workup
- customThe compound was synthesized
Sources & evidence
- ORD record
- ord-a9bc06e6da50413ab4e8ead32ac6474a
- Source dataset
- uspto-grants-2015_05
- Patent number
- US09034907B2
Reaction notes
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