HCID 4510667, compound → HCID 25100517, compound
Reaction equation
[N:1]([C:4]1[S:5][C:6]([CH3:19])=[C:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]=1[C:9]([O:11]C)=O)=[C:2]=[S:3].[CH3:20][C:21]1[N:22]=[CH:23][N:24]([CH2:26][CH2:27][CH2:28][NH2:29])[CH:25]=1>>[CH3:19][C:6]1[S:5][C:4]2[NH:1][C:2](=[S:3])[N:29]([CH2:28][CH2:27][CH2:26][N:24]3[CH:25]=[C:21]([CH3:20])[N:22]=[CH:23]3)[C:9](=[O:11])[C:8]=2[C:7]=1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1Participants
3
Procedure
The compound was synthesized starting from methyl 2-isothiocyanato-5-methyl-4-phenylthiophene-3-carboxylate (0.100 g. 0.35 mmol) and 3-(4-methyl-1H-imidazol-1-yl)propan-1-amine (9) (0.048 g, 0.35 mmol) as described above.
Workup
- customThe compound was synthesized
Sources & evidence
- ORD record
- ord-3dab25b6615442bcbc2ef1172404fed6
- Source dataset
- uspto-grants-2015_05
- Patent number
- US09034907B2
Reaction notes
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