methyl 3-isothiocyanatothiophene-2-carboxylate → HCID 25100819, compound

HRID 574730Notes

Reaction equation

HRID 574730 reaction equation
[N:1]([C:4]1[CH:8]=[CH:7][S:6][C:5]=1[C:9]([O:11]C)=O)=[C:2]=[S:3].[CH3:13][C:14]1[N:18]([CH2:19][CH2:20][CH2:21][NH2:22])[CH:17]=[N:16][CH:15]=1>>[CH3:13][C:14]1[N:18]([CH2:19][CH2:20][CH2:21][N:22]2[C:9](=[O:11])[C:5]3[S:6][CH:7]=[CH:8][C:4]=3[NH:1][C:2]2=[S:3])[CH:17]=[N:16][CH:15]=1

Participants

3

Reactant 2

HCID 2777461methyl 3-isothiocyanatothiophene-2-carboxylateHCID 194294833-(5-methyl-1H-imidazol-1-yl)propan-1-amine

Product 1

HCID 25100819HCID 25100819, compound

Procedure

The compound was synthesized starting from methyl 3-isothiocyanatothiophene-2-carboxylate (0.22 g, 1.08 mmol) and 3-(5-methyl-1H-imidazol-1-yl)propan-1-amine (5) (0.15 g, 1.08 mmol) as described above.

Workup

  1. customThe compound was synthesized

Sources & evidence

ORD record
ord-23fbc7eff0a24b1aba9a9f1f5716c224
Source dataset
uspto-grants-2015_05
Patent number
US09034907B2

Reaction notes

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