HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 2-isothiocyanato-, methyl ester → HCID 178515048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 2-isothiocyanato-, methyl ester | HCID 85243 | — |
| Reactant | HCID 178507353 | HCID 178507353 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178515048 | HCID 178515048 | — |
Reaction Steps
1H-benzo[d]imidazol-5-amine (0.14 g, 1.08 mmol) and methyl 2-isothiocyanatobenzoate (0.21 g, 1.08 mmol) were dissolved ind 10 mL of THF. The mixture was stirred by heating under reflux over night. The resulted insoluble solid was separated by suction through a frit and washed with THF to give a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09034907B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-b28db5be29f844f6933854bebe621c06 |
| Source note | uspto-grants-2015_05 |