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HRID575195

反应详情

EQUATION

反应方程式

HRID 575195 的结构方程式

REACTANTS

反应物

2
结构：NC(=O)c1cn2c(n1)-c1cc(Br)ccc1OCC2
HCID68312883

未命名化合物

结构：C#CC1(O)CCCN(C)C1=O
HCID86669576

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCCC(O)(C#Cc2ccc3c(c2)-c2nc(C(N)=O)cn2CCO3)C1=O
HCID86693201

未命名化合物

收率 17%

PROCEDURE

实验过程

Similar to as described in General Procedure G, 10-bromo-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide was reacted with 3-ethynyl-3-hydroxy-1-methylpiperidin-2-one (US2012/214762A1) to give the titled compound as a white solid (20 mg, 17%).