HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Ethynyl-3-oxetanol → HCID 86693217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Ethynyl-3-oxetanol | HCID 56777520 | — |
| Reactant | 10-Bromo-9-fluoro-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide | HCID 86693051 | — |
| Product | HCID 86693217 | HCID 86693217 | 83% |
Reaction Steps
Similar to as described in General Procedure G, 10-bromo-9-fluoro-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide was reacted with 3-ethynyloxetan-3-ol to give the titled compound as a light brown solid (140 mg, 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09034866B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-13929222849542edb542317f7c2349fc |
| Source note | uspto-grants-2015_05 |