HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanesulfonamide → US10023592, Example 169
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanesulfonamide | HCID 73702 | — |
| Reactant | US10023592, Example 149 | HCID 118022283 | — |
| Product | US10023592, Example 169 | HCID 118022284 | — |
Reaction Steps
The title compound of Example 149, step 4 was treated with EtSO2NH2 instead of MeSO2NH2 in a manner similar to Example 152, step 6 to give the title compound. 1H NMR (DMSO-d6, 400 MHz) δ 9.07 (s, 1H), 8.42 (s, 1H), 8.15 (s, 1H), 8.11 (s, 1H), 7.03-6.97 (m, 1H), 6.91-6.87 (m, 1H), 3.66-3.61 (m, 5H), 2.22 (s, 3H), 1.44 (t, J=7.6 Hz, 3H). LCMS: 437.0 (M+1)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09034900B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-73c477b06b5a46b59251343671f66b11 |
| Source note | uspto-grants-2015_05 |