HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 576018Generated: October 25, 2026
Ethylene Glycol → 2-Hydroxyethyl ethyl(3-aminopropyl)phosphinate
https://huagongshe.com/reaction/576018
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Butyl ethyl(3-aminopropyl)phosphinate | HCID 46212699 | — |
| Catalyst | Dipotassium;bis(2-hydroxy-2-oxoacetate);oxotitanium;hydrate | HCID 91886499 | — |
| Product | 2-Hydroxyethyl ethyl(3-aminopropyl)phosphinate | HCID 46212700 | 96% |
Reaction Steps
To 414 g (2 mol) of butyl ethyl(3-aminopropyl)phosphinate (produced as in Example 14) are added 155 g (2.5 mol) of ethylene glycol and 0.4 g of potassium titanyl oxalate and the mixture is stirred at 200° C. for 2 h. Gradual evacuation is applied to distill off volatiles, leaving 374 g (96% of theory) of 2-hydroxyethyl ethyl-(3-aminopropyl)phosphinate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09035088B2 |
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| Source dataset | uspto-grants-2015_05 |
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| ORD ID | ord-750eb5afa1e140ca816865f9ff42ca09 |
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| Source note | uspto-grants-2015_05 |
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