HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triphenylborane → Butyl ethyl(3-aminopropyl)phosphinate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triphenylborane | HCID 70400 | — |
| Edukt | Butyl ethyl(2-methyl-3-aminopropyl)phosphinate | HCID 46212766 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | Butyl ethyl(3-aminopropyl)phosphinate | HCID 46212699 | 216,6% |
Reaktionsschritte
207 g (1 mol) of butyl ethyl(3-aminopropyl)phosphinate (produced as in Example 15) and 242 g (1 mol) of triphenylborane are stirred in 400 ml of toluene at room temperature for 1 hour. Toluene is distilled off at reduced pressure to leave 449 g (100% of theory) of butyl ethyl(3-aminopropyl)phosphinate as triphenylborane adduct.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09035088B2 |
| Quelldatensatz | uspto-grants-2015_05 |
| ORD ID | ord-c43a7e6d12634605955e22ca7a853a9c |
| Quellennotiz | uspto-grants-2015_05 |