HCID 86714053, compound → HCID 89253561, compound

HRID 576386Notes

Reaction equation

ClC1C(CC2C=CC(OCC)=CC=2)=CC([C@H]2[C@H](OCC3C=CC=CC=3)[C@@H](OCC3C=CC=CC=3)[C@H](OCC3C=CC=CC=3)[C@@H](COCC3C=CC=CC=3)O2)=CC=1O.[CH2:58]([O:65][C@H:66]1[C@H:71]([O:72][CH2:73][C:74]2[CH:79]=[CH:78][CH:77]=[CH:76][CH:75]=2)[C@@H:70]([O:80][CH2:81][C:82]2[CH:87]=[CH:86][CH:85]=[CH:84][CH:83]=2)[C@H:69]([C:88]2[CH:93]=[C:92]([CH2:94][C:95]3[CH:100]=[CH:99][C:98]([O:101][CH2:102][CH3:103])=[CH:97][CH:96]=3)[C:91]([Cl:104])=[C:90]([O:105]C)[C:89]=2[O:107][CH3:108])[O:68][C@@H:67]1[CH2:109][O:110][CH2:111][C:112]1[CH:117]=[CH:116][CH:115]=[CH:114][CH:113]=1)[C:59]1[CH:64]=[CH:63][CH:62]=[CH:61][CH:60]=1>>[Cl:104][C:91]1[C:92]([CH2:94][C:95]2[CH:96]=[CH:97][C:98]([O:101][CH2:102][CH3:103])=[CH:99][CH:100]=2)=[CH:93][C:88]([C@H:69]2[C@H:70]([O:80][CH2:81][C:82]3[CH:87]=[CH:86][CH:85]=[CH:84][CH:83]=3)[C@@H:71]([O:72][CH2:73][C:74]3[CH:79]=[CH:78][CH:77]=[CH:76][CH:75]=3)[C@H:66]([O:65][CH2:58][C:59]3[CH:60]=[CH:61][CH:62]=[CH:63][CH:64]=3)[C@@H:67]([CH2:109][O:110][CH2:111][C:112]3[CH:113]=[CH:114][CH:115]=[CH:116][CH:117]=3)[O:68]2)=[C:89]([O:107][CH3:108])[C:90]=1[OH:105]

Participants

Reactant 2

HCID 86714053HCID 86714053, compound

HCID 90073514HCID 90073514, compound

Product 1

HCID 89253561HCID 89253561, compound

Procedure

Similar procedure with preparation of 77 proceeded except for using compound 162 to obtain the compound 163.

Sources & evidence

ORD record: ord-4472437e259b4dd6a8966f33a5052754
Source dataset: uspto-grants-2015_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09034921B2

Reaction notes

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