HCID 86714052, compound → HCID 90073618, compound

HRID 576390Notes

Reaction equation

[CH2:1]([O:8][C@H:9]1[C@H:14]([O:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[C@@H:13]([O:23][CH2:24][C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=2)[C@H:12](C2C=C(OC)C(Cl)=C(CC3C=CC(OCC)=CC=3)C=2)[O:11][C@@H:10]1[CH2:50][O:51][CH2:52][C:53]1[CH:58]=[CH:57][CH:56]=[CH:55][CH:54]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:59]([O:62][C:63]1[CH:68]=[C:67](Br)[CH:66]=[C:65]([CH2:70][C:71]2[CH:76]=[CH:75][CH:74]=[CH:73][CH:72]=2)[C:64]=1[Cl:77])[CH:60]=[CH2:61]>>[CH2:59]([O:62][C:63]1[CH:68]=[C:67]([C@H:12]2[C@H:13]([O:23][CH2:24][C:25]3[CH:26]=[CH:27][CH:28]=[CH:29][CH:30]=3)[C@@H:14]([O:15][CH2:16][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)[C@H:9]([O:8][CH2:1][C:2]3[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=3)[C@@H:10]([CH2:50][O:51][CH2:52][C:53]3[CH:54]=[CH:55][CH:56]=[CH:57][CH:58]=3)[O:11]2)[CH:66]=[C:65]([CH2:70][C:71]2[CH:76]=[CH:75][CH:74]=[CH:73][CH:72]=2)[C:64]=1[Cl:77])[CH:60]=[CH2:61]

Participants

Reactant 2

HCID 86714052HCID 86714052, compound

HCID 86714076HCID 86714076, compound

Product 1

HCID 90073618HCID 90073618, compound

Procedure

Similar procedure with preparation of 76 proceeded except for using compound 168 to obtain the compound 169.

Sources & evidence

ORD record: ord-790e711fb5b74970a0b012dce6a07457
Source dataset: uspto-grants-2015_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09034921B2

Reaction notes

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