HuagongsheHuagongshe Chemistry Print Report · For research reference only
Di-i-propylphosphine → 1,2-Bis(di-isopropylphosphinomethyl)ferrocene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Di-i-propylphosphine | HCID 536496 | — |
| Reactant | 1,2-Bis(dimethylaminomethyl)ferrocene | HCID 131727266 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 1,2-Bis(di-isopropylphosphinomethyl)ferrocene | HCID 131727271 | — |
Reaction Steps
The title compound was prepared in accordance with the procedure of Example 10 employing di-iso-propylphosphine (Digital Speciality Chemicals 392 mg, 3.33 mmol), 1,2-bis(dimethylaminomethyl)ferrocene (0.5 g, 1.66 mmol) and anhydrous acetic acid (100 ml). Yield 0.262 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040445B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-5cf6e897e58e43c3869bc3d26cfe0101 |
| Source note | uspto-grants-2015_05 |