HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-BOC-ethylenediamine → HCID 59313094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-BOC-ethylenediamine | HCID 187201 | — |
| Reactant | Methyl 2-[(tert-butoxycarbonyl)amino]-6-chloropyridine-3-carboxylate | HCID 53419545 | — |
| Product | HCID 59313094 | HCID 59313094 | — |
Reaction Steps
Analogously to the preparation of Example 33A, 650 mg (2.3 mmol) of methyl 2-[(tert-butoxycarbonyl)amino]-6-chloropyridine-3-carboxylate (Example 51A) and 363 mg (2.3 mmol) of N-Boc-ethylenediamine gave 500 mg (50% of theory) of the product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434731B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-0279ce9063a74591adb747c92f6887ab |
| Source note | uspto-grants-2016_09 |