HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Bromomethyl)-3,5-dichloropyridine → HCID 178516146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Bromomethyl)-3,5-dichloropyridine | HCID 22227766 | — |
| Reactant | HCID 178516148 | HCID 178516148 | — |
| Product | HCID 178516146 | HCID 178516146 | — |
Reaction Steps
This example was synthesized from 2-sulfanyl-6-(trifluoromethyl)pyrimidin-4-ol and 4-(bromomethyl)-3,5-dichloropyridine by following general procedure as described in the last step of Example 22. The title compound was obtained as a white solid (660 mg, 37% yield); 1H NMR (400 MHz, DMSO-d6): δ 4.72 (s, 2H), 6.69 (br, 1H), 8.64 (s, 2H); M+ 356.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040538B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-eaf012a0c49e4f41b83d6c34affffe2d |
| Source note | uspto-grants-2015_05 |