HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178429541, compound → HCID 178429529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178429541 | HCID 178429541 | — |
| Reactant | HCID 178478293 | HCID 178478293 | — |
| Product | HCID 178429529 | HCID 178429529 | — |
Reaction Steps
This example was synthesized from 3-(bromomethyl)-4-chloro-1H-pyrazole and 6-methyl-2-sulfanylpyrimidin-4-ol following general procedure as described in the last step of Example 22. The title compound was obtained as a white solid (500 mg, 20% yield); 1H NMR (400 MHz, DMSO-d6): δ 2.21 (s, 3H), 3.17 (s, 1H), 4.40 (s, 2H), 6.00 (bs, 1H), 7.93 (s, 1H); M+ 257.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040538B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-eb05698dee6c44739f5e513d23a48145 |
| Source note | uspto-grants-2015_05 |