HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 22499240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22499184 | HCID 22499184 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22499240 | HCID 22499240 | — |
Reaction Steps
To a solution of N-(2,5,6-trimethyl-indan-2-yl)-benzamide in THF under nitrogen is added LiAlH4 and the mixture refluxed for 48 hours. Quenched at 0° C. with ice/water and extracted with ether, dried (Na2SO4) and solvent removed in vacuo. Purification by chromatography (silica, ethyl acetate/hexane 1:4) gives a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040559B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-31fdc33c8ad642eabda3cfef8976de99 |
| Source note | uspto-grants-2015_05 |