HCID 86679686, compound → HCID 86679685, compound

Participants

Reaction Steps

To a solution of tert-butyl(cis)-5-benzyl-3a-[(tert-butoxycarbonyl)oxy]hexahydropyrrolo[3,4-c]pyrrole-2(1H)-carboxylate (274 mg, 0.861 mmol) in EtOH (8.61 mL) purged with nitrogen was added Pd(OH)2/C (27 mg) and the resulting mixture stirred under a H2 balloon for 18 hrs. The reaction mixture was filtered and then concentrated under reduced pressure to obtain the crude title compound that was carried forward to the next step without further purification. m/z (APCI+) for C16H28N2O5 429.20 (M+H)+.

Provenance & Evidence