HCID 67231343, compound → HCID 67230443, compound

HRID 578066Notes

Reaction equation

HRID 578066 reaction equation
[NH2:1][C:2]1[C:10]([N+:11]([O-])=O)=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[C:4]([O:14][CH2:15][C:16]([F:19])([F:18])[F:17])[CH:3]=1>[Pd].CO>[NH2:1][C:2]1[C:10]([NH2:11])=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[C:4]([O:14][CH2:15][C:16]([F:17])([F:18])[F:19])[CH:3]=1

Participants

4

Reactant 1

HCID 67231343HCID 67231343, compound

Product 1

HCID 67230443HCID 67230443, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

Prepared analogously to example 655d from the product obtained in (675c) by hydrogenation using palladium on charcoal in methanol.

Workup

  1. customPrepared analogously to example 655d from the product

Sources & evidence

ORD record
ord-96e85782ec6d4a908e11147327f8a189
Source dataset
uspto-grants-2015_05
Patent number
US09040565B2

Reaction notes

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