Ammonia → HCID 2032425, compound

HRID 578190Notes

Reaction equation

HRID 578190 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([OH:12])=O)=[CH:9][C:4]=2[O:3][CH2:2]1.O[N:14]=[C:15]([NH2:22])[C:16]1[CH:21]=[CH:20][CH:19]=[N:18][CH:17]=1.N>>[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]3[O:12][N:22]=[C:15]([C:16]4[CH:17]=[N:18][CH:19]=[CH:20][CH:21]=4)[N:14]=3)=[CH:9][C:4]=2[O:3][CH2:2]1

Participants

4

Reactant 3

HCID 222AmmoniaHCID 71961,3-Benzodioxole-5-carboxylic acidHCID 308113N-Hydroxynicotinimidamide

Product 1

HCID 2032425HCID 2032425, compound

Procedure

The title compound was prepared according to method C using benzo[d][1,3]dioxole-5-carboxylic acid (Aldrich) and N′-hydroxynicotinimidamide (Tyger). 1H NMR (300 MHz, DMSO-d6) δ 6.22 (s, 2H), 7.20 (d, J=8.1 Hz, 1H), 7.61-7.69 (m, 2H), 7.81 (dd, J=8.1, 1.7 Hz, 1H), 8.42 (dt, J=8.2, 1.9, 1.7 Hz, 1H), 8.81 (dd, J=4.7, 1.7 Hz, 1H), 9.24 (dd, J=2.2, 0.8 Hz, 1H) ppm; MS (DCI/NH3) m/z 268 (M+H)+.

Sources & evidence

ORD record
ord-e8ce0cc318da4cb8b624f051a02062ef
Source dataset
uspto-grants-2015_05
Patent number
US09040568B2

Reaction notes

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